Abstract
Suxamethonium chloride in dog meat was extracted by ultrasonic vibration with Na2CO3—NaHCO3 buffer solution，then the supernatant was cleaned-up using WCX solid phase extraction cartridges. The qualitative and quantitative analysis for target was achieved by liquid chromatography-tandem mass spectrometry. The study showed that the suxamethonium chloride concentration had a good linear relationship (r=0.999 87)with mass signal ranging from 0.5～250.0 ng/mL. The recovery was above 96%. The relative standard deviation was below 13%. The limit of determination was 0.004 mg/kg. This is a rapid, sensitive, accurate method for determinating suxamethonium chloride in dog meat.
Publication Date
12-28-2015
First Page
102
Last Page
104
DOI
10.13652/j.issn.1003-5788.2015.06.023
Recommended Citation
Xingwang, ZHOU; Shaoying, KANG; Jihong, ZHANG; and Qiao, ZOU
(2015)
"Determination of suxamethonium chloride in meat by HPLC—MS／MS method,"
Food and Machinery: Vol. 31:
Iss.
6, Article 23.
DOI: 10.13652/j.issn.1003-5788.2015.06.023
Available at:
https://www.ifoodmm.cn/journal/vol31/iss6/23
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