Abstract
The organophosphorus pesticide is still widely used in agricultural production, organophosphorus pesticide and its metabolites have more severe toxic to the human body. This paper details the organophosphorus pesticide residues in fruits and vegetables analysis detection technology at home and abroad, and the prospect on the development of organophosphorus pesticide residue detection was discussed.
Publication Date
2-28-2016
First Page
173
Last Page
177,182
DOI
10.13652/j.issn.1003-5788.2016.02.042
Recommended Citation
Yajia, ZHANG and Zhonghai, LI
(2016)
"Research progress on detection methods for organophosphorus pesticide in fruits and vegetables,"
Food and Machinery: Vol. 32:
Iss.
2, Article 42.
DOI: 10.13652/j.issn.1003-5788.2016.02.042
Available at:
https://www.ifoodmm.cn/journal/vol32/iss2/42
References
[1] 吴武杰, 保志娟, 权小菁, 等. 有机磷农药残留检测前处理技术研究进展[J]. 化学分析计量, 2009, 18(4): 88-89.
[2] 林春绵, 胡晓燕, 张安平. 酶抑制法快速检测有机磷农药残留的研究进展[J]. 浙江工业大学学报, 2009, 37(4): 386-391.
[3] 曾家源, 黄俊硕. 有机磷农药检测方法的研究进展[J]. 广东化工, 2015, 42(5): 70-71.
[4] 江英志, 谢桂勉. 有机磷农药多残留检测研究进展[J]. 安徽农业科学, 2010, 38(17): 9 060-9 061, 9 192.
[5] 朱贺, 纪明山. 农药残留快速检测方法的研究进展[J]. 中国农学通报, 2014, 30(2): 242-250.
[6] 薛平, 史惠娟, 杜利君, 等. 5种基质中19种有机磷农药残留的基质固相分散—气相色谱法测定[J]. 食品科学, 2010, 31(18): 227-231.
[7] 王玲莉, 廖云华, 舒丽萍, 等. 2007—2008年杭州市非生产性急性农药中毒情况分析[J]. 中国预防医学杂志, 2010, 11(4): 379-380.
[8] 林春绵, 胡晓燕, 张安平. 酶抑制法快速检测有机磷农药残留的研究进展[J]. 浙江工业大学学报, 2009, 37(4): 386-391.
[9] 何丽芳, 王芳宇, 邹征. 衡阳市蔬菜水果农药残留现状、原因与对策[J]. 衡阳师范学院学报, 2012, 33(3): 82-85.
[10] 易承学, 徐虹, 蒲彦利, 等. 2014年镇江市夏季蔬菜农药残留检测分析[J]. 职业与健康, 2015, 31(3): 326-327.
[11] 孙中强, 吉莉丽, 胡美华, 等. 2013年江西省蔬菜中21种农药残留状况调查[J]. 现代预防医学, 2014, 24(41): 4 443-4 444.
[12] 韦江峰, 李翔, 胡支向, 等. 柑橘中有机磷类农药使用调查初探[J]. 农业与技术, 2015, 4(35): 36-37.
[13] 李俊杰, 侯长军, 霍丹群, 等. 有机磷农药快速检测方法与技术进展[J]. 食品安全质量检测学报, 2013, 4(1): 19-26.
[14] Vongsvivut Jitraporn, Robertson Evan G, McNaughton Don. Surface-enhancesed Raman spectroscopic analysis of fonofos pesticide adsorbed on silver and gold nanoparticles[J]. Journal of Raman Spectroscopy, 2010, 41(10): 1 137-1 148.
[15] 沈飞, 闫战科, 叶尊忠, 等. 近红外光谱分析技术在辛硫磷农药残留检测中的应用[J]. 光谱学与光谱分析, 2009, 29(9): 2 421-2 424.
[16] 季仁东, 赵志敏, 张林, 等. 苹果汁中吡虫啉农药残留荧光检测研究[J]. 光谱学与光谱分析, 2013, 12(6): 668-671.
[17] 陈丹萍, 王乐新, 高天祎. 蔬菜中丙森锌农药残留的吸收光谱检测[J]. 安徽农业科学, 2015, 43(12): 130-131.
[18] 杜鹃. 果蔬中有机磷农药残留检测方法的研究进展[J]. 广东化工, 2012, 39(9): 153-155.
[19] Cao Hai-qun, Yue Yong-de, Hua Ri-mao, et al. HPTLC determination of imidacloprid, fenitrothion and parathion in Chinese cabbage[J]. J. Planar Chromatogr-Mod TLC, 2005, 18(102): 151-154.
[20] Li Ling, Zhou Shan-shan, Jin Li-xia, et al. Enantiomeric separation for organopho sphorus pesticides by high performance liquid chromatography, gas chromatography and capillary electrophoresis and their application in environmental behavior and toxicity assay[J]. Journal of Chromatography B, 2010, 878(17): 1 264-1 276.
[21] Su Rui, Xu Xu, Wang Xing-hua, et al. Determination of organophosphorus pesticides in peanut oil by dispersive solid phase extraction gas chromatography-mass spectrometry[J]. Journal of Chromatography B, 2011, 879(30): 3 423-3 428.
[22] Akkad R, Schwack W. Multi-enzyme inhibition assay for the detection of insecticidal organophosphates and carbamates by high-performance thin-layer chromatography applied to determine enzyme inhibition factors and residues in juice and water samples[J]. Journal of Chromatography B, 2010, 87(15): 1 337-1 345.
[23] 陈道勇, 杨略, 郭嘉, 等. 有机磷农药残留的分析检测及最新研究进展[J]. 中国粮油学报, 2011, 28(11): 7-12.
[24] 陈文强, 彭浩, 邓百万, 等. 气相色谱技术在食品安全检测中的应用[J]. 江苏农业科技, 2009(4): 356-358.
[25] Zhang Shan-qing, Zhao Hui-jun, John R. Development of a quantitative relationship between inhibition percentage and both incubation time and inhibitor concentration for inhibition biosensors-theoretical and practical considerations [J]. Biosens Bioelectron, 2001, 5(16): 1 119-1 121.
[26] 齐强, 黄志仁. 改良QuEChERS—气相色谱法测定苹果中7种有机磷类农药残留[J]. 广东化工, 2014(19): 67-72.
[27] 刘兰侠, 张燕, 陈翔, 等. CGC-FPD测定生活饮用水中痕量有机磷农药的研究[J]. 中国卫生检验杂志, 2014(5): 644-646.
[28] 南京熙, 毕程程, 金京一, 等. 超声萃取—气流式液相微萃取—气相色谱质谱在线联用快速检测蔬菜中有机磷农药残留[J]. 食品与机械, 2014, 30(5): 72-82.
[29] 王桂才. 油菜籽中有机磷农药多残留分析方法研究[D]. 北京: 中国农业科学院, 2006: 27-29.
[30] Kim D H, Heo G S, Lee D W. Determination of organophosphorus pesticides in wheat flour by supercritical fluid extraction and gas chromatography with mtrogen-phoosphorus detection[J]. Journal of Chromatograph, 1998, 824(1): 63-70.
[31] 张潜, 高玲, 赖发伟, 等. 电子捕获检测器—气相色谱法测定饮用水中多种有机磷残留[J]. 现代预防医学, 2007, 34(14): 2 715-2 717.
[32] Albero B, Sanchez B C, Tadeo J L. Determination of organophosphorus pesticides in fruit juices by matrix solid-phase dispersion and gas chromatography[J]. Journal of Agricultural and Food Chemistry, 2003, 51(24): 6 915-6 921.
[33] 王红章. 气相色谱快速测定土壤中的有机磷农药[J]. 福建地质, 2012, 10(3): 284-287.
[34] 武开业. 气相色谱质谱联用仪的原理及分类[J]. 科技视界, 2009, 12(3): 270.
[35] 幸红星. 有机磷类农药残留检测技术的应用[J]. 分析测试技术与仪器, 2012, 18(4): 234-238.
[36] Wong Jing-wang, Zhang Ke, Tech K, et al. Muitiresidue pesticide analysis in fresh produce by capillary gas chromatography-mass spectrometry/selective ion monitoring(GC—MS/SIM) and tandem mass spectrometry(GC—MS/MS) [J]. Journal of Agricultural and Food Chemistry, 2010, 58(10): 5 868-5 883.
[37] 王海凤, 王俊斌, 刘海学, 等. 气质联用法同时测定果蔬中多种有机磷农药残留[J]. 食品与机械, 2013, 29(1): 92-94.
[38] Cortada C, Vidalb L, Tejada S. Determination of organochlorine pesticides in complex matrices by single-drop microextraction coupled to gas chromatogramphy-mass spectrometry[J]. Analytica Chimica Acta, 2009, 638(12): 29-35.
[39] Dos Anjos J P, de Andrade J B. Determination of nineteen pesticides residues (organophosphates, organochlorine, pyrethroids, carbamate, thiocarbamate and strobilurin) in coconut water by SDME/GC—MS[J]. Microchemical Journal, 2014, 112(5): 119-126.
[40] 张玉美, 曾红燕, 罗靖, 等. QuEChERS—气相色谱质谱法检测蔬菜中的34种农药残留[J]. 预防医学情报杂志, 2015, 5(31): 375-377.
[41] Chen Hao, Chen Rui-wen, Feng Rui. Simultaneous analysis of carbamate and organophosphorus pesticides in water by single-drop microextraction coupled with GC—MS[J]. Chromatographia, 2009, 70(1/2): 165-172.
[42] Seebunrueng K, Santaladchaiyakit Y, Srijaranai S. Vortex-assisted low density solvent liquid-liquid microextraction and salt-induced demulsification coupled to high performance liquid chromatography for the determination of five organophosphorus pesticide residues in fruits[J]. Talanta, 2015, 132(1): 769-774.
[43] Seebunrueng K, Santaladchaiyakit Y, Srijaranai S. Vortex-assisted low density solvent based demulsified dispersive liquid-liquid microextraction and high-performance liquid chromatography for the determination of organophosphorus pesticides in water samples[J]. Chemosphere, 2014, 103(5): 51-58.
[44] 陈芳, 杨冰仪, 龙军标, 等. 有机磷农药残留检测的研究进展[J]. 中国卫生检验杂志, 2007, 17(2): 382-384.
[45] 邵金良, 刘宏程, 梅文泉, 等. 基质固相分散萃取—HPLC分析番茄中6种农药残留[J]. 食品与机械, 2013, 29(1): 67-70.
[46] 郑春慧, 杨立刚, 姚志云, 等. 白菜中有机磷农药的电纺纳米纤维固相萃取—高效液相色谱法测定[J]. 分析测试学报, 2009, 28(8): 926-930.
[47] Xu Zi-xiang, Fang Guo-zhen, Wang Shuo. Molecularly imprinted solid phase extraction coupled to high-performance liquid chromatography for determination of trace dichlorvos residues in vegetables[J]. Food Chemistry, 2010, 119(2): 845-850.
[48] Henry K Rotich. 环境水中甲基对硫磷、对硫磷和辛硫磷农药残留的SPE—HPLC分析[J]. 分析测试学报, 2002, 21(5): 50-53.
[49] 甘宾宾, 汤艳荣, 蒋世琼. 高效液相色谱—质谱联用技术在食品安全中的应用及进展[J]. 化工技术与开发, 2009, 38(12): 33-37.
[50] Hassjy J. Rapid and simple low density miniaturized homogeneous liquid-liquid extraction and gas chromatography/mass spectrometric determination of pesticide residues in sediment[J]. Journal of Hazardous Materials, 2010, 184(1/2/3): 869-871.
[51] Wang Ying, Jin Hong-yu, Ma Shuang-cheng. Determination of 195 pesticide residues in Chinese herbs bygas chromatography-mass spectrometry using analyte protectants[J]. Journal of Chromatography A, 2011, 1 218(2): 334-342.
[52] Osman K A, AL-Humaid A I, Al-Rehiayani S M, et al. Estimated daily intake of pesticide residues exposure by vegetables grown in greenhouses in al-qassim Region, Saudi Arabia[J]. Food Control, 2011, 22(6): 947-953.
[53] Kujawski. Levels of 13 multi-class pesticide residues in Polish honeys determined by LC—ESI—MS/MS[J]. Food Control, 2011, 22(6): 914-919.
[54] 晏利芝, 赵永彪, 刘宁, 等. UPLC—MS/MS法同时测定蔬菜中34种农药残留[J]. 食品研究与开发, 2015, 36(3): 100-103.
[55] Arienzo M, Cataldo D, Ferrara L. Pesticide residues in fresh-cut vegetables from integrated pest management by ultra performance liquid chromatography coupled to tandem mass spectrometry[J]. Food Control, 2013, 5(31): 108-115.
[56] Xu Zhen-lin, Deng Hao, Deng Xing-fei, et al. Monitoring of organophosphorus pesticides in vegetables using monoclonal antibody-based direct competitive ELISA followed by HPLC—MS/MS[J]. Food Chemistry, 2012, 131(4): 1 569-1 576.
[57] 林涛, 邵金良, 刘兴勇, 等. 超高效液相色谱—串联质谱法测定蔬菜中41种农药残留[J]. 色谱, 2015, 33(3): 235-241.
[58] Carneiro R P, Oliveira F A S. Development and method validation for determination of 128 pesticides in bananas by modified QuEChERS and UHPLC—MS/MS analysis[J]. Food Control, 2013, 33(12): 413-423.
[59] Campanella L, Bonanni A, Martini E, et al. Determination of triazine pesticides using a new enzyme inhibition tyrosinase OPEE operating in chloroform[J]. Sensors and Actuators B: Chemical, 2005, 111-112(11): 505-514.
[60] 吴丽华. 苹果中多种农药残留的分析检测方法研究[D]. 西安: 陕西师范大学, 2007, 24(5): 33-38.
[61] 桑园园, 柴丽娜, 魏朝俊, 等. 酶抑制法检测4种辛辣蔬菜农药残留假阳性消除的研究[J]. 中国农学通报, 2009, 25(11): 60-64.
[62] Nagatani N, Takeuchi A, Hossain M A, et al. Rapid and sensitive visual detection of residual pesticides in food using acetylcholine esterase-based disposable membrane chips[J]. Food Control, 2007, 18(8): 914-920.
[63] 邱朝坤, 刘晓宇, 任红敏, 等. 酶抑制法检测蔬菜中有机磷农药残留[J]. 食品与机械, 2010, 26(2): 40-42.
[64] Alina C I, Ion I, Alina C, et al. Acetylcholinesterase voltammetric biosensors based on carbon nanostructurechitosan composite material for organophosphate pesticides[J]. Materials Science and Engineering C, 2010, 30: 817-821.
[65] 武中平, 徐春祥, 高巍, 等. 酶联免疫分析法及其在食品农药残留检测中的应用[J]. 江苏农业科学, 2007(1): 198-201.
[66] Dalvie M A, Sinanovic E, London L, et al. Cost analysis of ELISA, solid-phase extraction, and solid-phase microextraction for the monitoring of pesticides in water[J]. Environmental Research, 2005, 98(1): 143-150.
[67] Joshi K A, Tang J, Haddon R, et al. A disposable biosensor for organophosphorus herve agents based on carbon nanotubes modified thick film strip electrode[J]. Electroanalysis, 2005, 17(1): 54-58.
[68] Wang Lei, Zhang Li-jie, Li Wei, et al. Determination of organophosphorus pesticides based on biotin-avidin enzyme-linked immunosorbent assay[J]. Chinese Journal of Analytical Chemistry, 2011, 39(3): 346-350.
[69] Qian Guo-liang, Wang Li-ming, Wu Yun-ru, et al. A monoclonal antibody-based sensitive enzyme-linked immunosorbent assay (ELISA) for the analysis of the organophosphorous pesticides chlorpyrifos-methyl in real samples[J]. Food Chemistry, 2009, 117(2): 364-370.
[70] 韩波, 姚安庆, 王勇, 等. 应用植物酯酶测定农药残留研究进展[J]. 长江大学学报: 自然科学版, 农学卷, 2009, 6(3): 60-65.
[71] 王莉, 李锋, 姚冰, 等. 以DTNB为电子媒介检测农产品中甲拌磷残留的生物传感法的建立[J]. 食品科技, 2010(12): 312-315.
[72] Kumaravel A, Chandrasekaran M. A novel nanosilver/nafion composite electrode for electrochemical sensing of methyl parathion and parathion[J]. Journal of Electroanalytical Chemistry, 2010, 638(2): 231-235.
[73] Kumaravel A, Chandrasekran M. A biocompatible nano TiO2/nafion composite modified glassy carbon electrode for the detection of fenitrothion[J]. Journal of Electroanalytical Chemistry, 2011, 650(2): 163-170.
[74] 伍周玲, 燕冰宇, 梁东军, 等. 新型固载酶生物传感器制备及食品中有机磷农药检测[J]. 中国食品学报, 2015, 15(3): 166-173.