Separation of citral from Litsea Cubeba oil by phase transfer catalysis

Authors

FU Hongjun, College of Food Science and Engineering, Central South University of Forestry and Technology, Changsha, Hunan 410004, China; National Engineering Laboratory for Rice and Byproducts Processing, Changsha, Hunan 410004, China
PENG Xianglian, College of Food Science and Engineering, Central South University of Forestry and Technology, Changsha, Hunan 410004, China; National Engineering Laboratory for Rice and Byproducts Processing, Changsha, Hunan 410004, China
KUANG Chuntao, College of Material Science and Engineering, Central South University of Forestry and Technology, Changsha, Hunan 41004, China
ZHONG Haiyan, College of Food Science and Engineering, Central South University of Forestry and Technology, Changsha, Hunan 410004, China; National Engineering Laboratory for Rice and Byproducts Processing, Changsha, Hunan 410004, China

Abstract

Randomly methylated- β-cyclodextrin (RM-β-CD) was used as phase transfer catalysis to separate citral from Litsea cubeba oil by addition reaction and hydrolysis reaction. The optimum separation conditions were obtained by single factor experiment design and Box-Behnken experiment design. The purity and yield of citral were 96.50% and 86.60%, respectively, which was gotten under the optimum conditions of reaction time 3.3 h, RM-β-CD amount 0.65% (molar fraction) and reaction temperature 15.0 ℃. Predicted value was in accordance with actual value. This proposed method was used to separate citral from Litsea cubeba oil with convenient and had high efficient advantages.

Publication Date

9-28-2016

First Page

161

Last Page

165,186

DOI

10.13652/j.issn.1003-5788.2016.09.039

Recommended Citation

Hongjun, FU; Xianglian, PENG; Chuntao, KUANG; and Haiyan, ZHONG (2016) "Separation of citral from Litsea Cubeba oil by phase transfer catalysis," Food and Machinery: Vol. 32: Iss. 9, Article 39.
DOI: 10.13652/j.issn.1003-5788.2016.09.039
Available at: https://www.ifoodmm.cn/journal/vol32/iss9/39

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