Extraction optimization of enzyme hydrolysis method and GC-MS analysis on oleoresin from Zanthoxylum

Authors

CHAI Liqin, College of Food Engineering and Nutritional Science of Shaanxi Normal University, Xi’an, Shaanxi 710119, China
YUAN Hong, College of Food Engineering and Nutritional Science of Shaanxi Normal University, Xi’an, Shaanxi 710119, China
WANG Lixia, College of Food Engineering and Nutritional Science of Shaanxi Normal University, Xi’an, Shaanxi 710119, China
LU Yuehong, College of Food Engineering and Nutritional Science of Shaanxi Normal University, Xi’an, Shaanxi 710119, China
TIAN Chengrui, College of Food Engineering and Nutritional Science of Shaanxi Normal University, Xi’an, Shaanxi 710119, China

Abstract

Zanthoxylum was used as the material. Combined cellulase hydrolysis with response surface method to optimize the Zanthoxylum oleoresin (Z瘙簚oleoresin) extraction process. Results showed that the optimum extraction conditions of Z瘙簚oleoresin as follows: 50% ethanol as extractant, cellulase dosage was 62.3 mg/L, enzymolysis time was 2.3 h, enzymolysis temperature was 50 ℃, liquid ratio was 47.41(mL/g). In this condition, the extraction efficiency of Z瘙簚oleoresin was 37.22%. A total of 47 compounds were identified by gas chromatography-mass spectrometry (GC-MS). Main ingredients were D-limonene, linalool, lauricacid, limonene glycol, alpha-terpineol, ascaridole, citronellyl myristate, xanthoxylin, etc.

Publication Date

9-28-2017

First Page

162

Last Page

166,172

DOI

10.13652/j.issn.1003-5788.2017.09.034

Recommended Citation

Liqin, CHAI; Hong, YUAN; Lixia, WANG; Yuehong, LU; and Chengrui, TIAN (2017) "Extraction optimization of enzyme hydrolysis method and GC-MS analysis on oleoresin from Zanthoxylum," Food and Machinery: Vol. 33: Iss. 9, Article 34.
DOI: 10.13652/j.issn.1003-5788.2017.09.034
Available at: https://www.ifoodmm.cn/journal/vol33/iss9/34

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