Determination of theresidual volatile phenols in fish meat and its products by the flow injection spectrophotometric

Authors

Yin-qi CHENG, Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075 , China ；HubeiProvincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan,Hubei 430075 , China
Xin ZHENG, Wuhan Center Testing International Co., Ltd., Wuhan, Hubei 430223 , China
Di LIU, Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075 , China ；HubeiProvincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan,Hubei 430075 , China
Hao FENG, Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075 , China ；HubeiProvincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan,Hubei 430075 , China
Ying ZHU, Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075 , China ；HubeiProvincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan,Hubei 430075 , China
Qing-zhi PENG, Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075 , China ；HubeiProvincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan,Hubei 430075 , China
Tao-hong ZHOU, Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075 , China ；HubeiProvincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan,Hubei 430075 , China

Abstract

Using flow injection analysis technology, online distillation, extraction, and color development, a continuous flow analysis method for rapid determination of volatile phenol residues in fish meat and its products was established. The results showed that the linear range of the established detection method was 0.00~40.00 μg/L, with the correlation coefficient r=0.999 9, the detection limit of the method is 0.030 mg/kg, with the RSD ranging from 0.952% to 6.543% (n=11). The standard recovery rate was 72.000%~90.827%. Compared with the standard method, this method had the advantages of accuracy, efficiency, simplicity, and environmental protection, and was suitable for the promotion and application of testing institutions and production enterprises.

Publication Date

2-18-2023

First Page

49

Last Page

52,86

DOI

10.13652/j.issn.1003-5788.2020.10.010

Recommended Citation

CHENG, Yin-qi; ZHENG, Xin; LIU, Di; FENG, Hao; ZHU, Ying; PENG, Qing-zhi; and ZHOU, Tao-hong (2023) "Determination of theresidual volatile phenols in fish meat and its products by the flow injection spectrophotometric," Food and Machinery: Vol. 36: Iss. 10, Article 10.
DOI: 10.13652/j.issn.1003-5788.2020.10.010
Available at: https://www.ifoodmm.cn/journal/vol36/iss10/10

References

[1] 中国水产科学研究院环保室.2000年中国渔业环境预测[R].北京:中国水产科学研究院环保室,1989:6-30.
[2] 王红梅.挥发酚对鲫生理指标的影响及其检测与降解研究[D].武汉:华中农业大学,2011:19-20.
[3] 杨利娴.流动注射分析法测定挥发酚考核样探讨[J].广东化工,2019,46(21):129-130.
[4] 夏文盛.SKALAR连续流动分析仪测定地表水中的挥发酚[J].环境与发展,2020,32(1):172-173.
[5] 黄贤伟.流动注射在线蒸馏法测定水中挥发酚[J].能源与环境,2019(4):93-94.
[6] 战培荣,王海涛,陈中祥,等.鱼体中挥发酚的提取与残留分析[J].农业环境科学学报,2008(2):801-804.
[7] 罗宏德,葛振平,尹杰,等.流动注射—光度法测定地表水中挥发[J].理化检验,2007,43(10):841-843
[8] 桂婷婷,朱兆中,王慧,等.全自动流动注射法测定餐(饮)具表面残留阴离子合成洗涤剂[J].中国卫生检验杂志,2020,30(2):148-150.
[9] SOUSA F M,FERREIRA R J R,S S V M,et al.Novel analytical approach to assess the profile of volatile phenols in Portuguese red wines[J].Australian Journal of Grape and Wine Research,2020,26(1):90-100.
[10] MCKAY M,BAUER F F,PANZERI V,et al.Perceptual interactions and characterisation of odour quality of binary mixtures of volatile phenols and 2-isobutyl-3-methoxypyrazine in a red wine matrix[J].Journal of Wine Research,2020,31(1):49-66.
[11] 张敏,甘瑛琳,吴恩宁,等.连续流动注射分析法同时测定水中挥发酚、氰化物及阴离子合成洗涤剂[J].医学动物防制,2020,36(4):404-407.
[12] 陈慧玲,毛丽莎,许欣欣,等.间隔流动分析法同时检测生活饮用水中的挥发酚类和氰化物[J].食品安全质量检测学报,2019,10(20):6 997-7 000.
[13] 柴丽月,钟惠英,柳海,等.宁波市水产品中挥发酚含量分析[J].中国渔业质量与标准,2015,5(1):61-65.
[14] 王红梅,李小定,熊善柏,等.直接蒸馏/4-氨基安替比林法检测淡水鱼体内挥发酚的含量[J].食品科学,2011,32(4):196-199.
[15] 林凯,罗若荣,陈裕华,等.间隔流动注射分析仪测定鱼中挥发酚的实验研究[J].职业与健康,2009,25(9):925-926.
[16] 罗若荣,林凯,陈方舟,等.深圳市不同鱼体中挥发酚污染及评价[J].中国公共卫生,2008(6):689-690.