Abstract
Objective:The flavor formation process of stewed pork was investigated in this study. Methods: Electronic nose and gas-phase mass spectrometry (GC-MS) techniques were used to compare the key processes such as bleaching, frying, stewing and addition of sauces during the processing of stewed pork, and to analyze the changes of flavor compounds. Results: The results of electronic nose measurement were consistent with the results of gas chromatography analysis. The flavor content of raw pork and sauces was the highest, and the flavor substances decreased in the blanching, frying and stewing stages. However, the characte-ristic flavor substances were formed continuously. A total of 148 compounds were detected by GC-MS, including 39, 32, 23, 20, 38, and 65 compounds in raw pork, blanched, fryed, stewed and finished products and sauces, respectively, which mainly produced aldehydes and ketones, esters and alcohols, heterocyclic compounds, and aromatic hydrocarbons and their derivatives. The characteristic flavors of finished products were hexanal, benzaldehyde, 1-octen-3-ol, cinnamaldehyde, 2-pentylfuran, 2-acetyl pyrrole, 2,3-dimethyl-5-ethylpyrazine, etc. The content of acetoin was higher in the pre-preparation stage of stewed pork, while methoxy-phenyl-Oxime stayed high in all of the processes. Conclusion: The electronic nose technique can be used to detect the changes of flavor substances in different processing stages of stewed pork, but the specific substance changes need to be determined and analyzed by GC-MS.
Publication Date
7-4-2022
First Page
13
Last Page
21
DOI
10.13652/j.issn.1003-5788.2022.01.002
Recommended Citation
Min, YAO; Guo-fang, XIE; Rong, YANG; Di, ZHOU; Qing-meng, LONG; and Chun-jiang, ZHANG
(2022)
"Analysis of flavor compounds in the process of stewed pork at key stages,"
Food and Machinery: Vol. 38:
Iss.
1, Article 2.
DOI: 10.13652/j.issn.1003-5788.2022.01.002
Available at:
https://www.ifoodmm.cn/journal/vol38/iss1/2
References
[1] 黄业传,贺稚非,李洪军,等.皮下脂肪和肌内脂肪对猪肉风味的作用[J].中国农业科学,2011,44(10):2 118-2 130.HUANG Ye-chuan,HE Zhi-fei,LI Hong-jun,et al.The flavor contribution of subcutaneous and intramuscular fat to pork[J].Scientia Agricultura Sinica,2011,44(10):2 118-2 130.
[2] 张春江,张良,黄峰,等.中式肉类菜肴加工中营养品质变化研究进展[J].生物产业技术,2017(4):76-81.ZHANG Chun-jiang,ZHANG Liang,HUANG Feng,et al.Progress of research on nutritional quality changes in the processing of Chinese meat dishes[J].Bioindustry Technology,2017(4):76-81.
[3] 潘见,杨俊杰,邹英子.不同涂层SPME与GC-MS联用比较分析两种猪肉挥发性风味成分[J].食品科学,2012,33(12):169-172.PAN Jian,YANG Jun-jie,ZOU Ying-zi.Comparative analysis of flavor components in Pork from different breeds by SPME with different fiber coatings and GC-MS[J].Food Science,2012,33(12):169-172.
[4] 刘莉丹,黄峰,周芳伊,等.三种红烧肉挥发性风味成分的比较研究[J].食品工业科技,2019,40(13):141-147.LIU Li-dan,HUANG Feng,ZHOU Fang-yi,et al.Comparative study on volatile flavor components of three kinds of braised pork meats[J].Science and Technology of Food Industry,2019,40(13):141-147.
[5] 朱文政,严顺阳,徐艳,等.顶空固相微萃取—气质联用分析不同烹制时间红烧肉挥发性风味成分[J].食品与发酵工业,2021,47(2):247-253.ZHU Wen-zheng,YAN Shun-yang,XU Yan,et al.Analysis of volatile flavor components of braised pork with different cooking time by SPME-GC-MS[J].Food and Fermentation Industries,2021,47(2):247-253.
[6] 王瑞花,姜万舟,汪倩,等.红烧猪肉工艺优化及其挥发性风味成分的分离与鉴定[J].中国食品学报,2017,17(5):208-216.WANG Rui-hua,JIANG Wan-zhou,WANG Qian,et al.Process optimization of braised pork and isolation and identification of its volatile flavor components[J].Journal of Chinese Institute of Food Science and Technology,2017,17(5):208-216.
[7] 史笑娜,黄峰,张良,等.红烧肉加工过程中脂肪降解、氧化和挥发性风味物质的变化研究[J].现代食品科技,2017,33(3):257-265.SHI Xiao-na,HUANG Feng,ZHANG Liang,et al.Changes in lipolysis,lipid oxidation,and volatile flavor compounds during the processing of red braised pork[J].Modern Food Science and Technology,2017,33(3):257-265.
[8] 顾伟钢,张进杰,姚燕佳,等.红烧肉制作过程中脂肪氧化和脂肪酸组成的变化[J].食品科学,2011,32(17):76-80.GU Wei-gang,ZHANG Jin-jie,YAO Yan-jia,et al.Lipid oxidation and fatty acid composition change during the processing of stewed pork[J].Food Science,2011,32(17):76-80.
[9] 范丽,徐晓东,宋泽,等.自制调味汁烹饪红烧肉中关键香气活性化合物的分析研究[J].现代食品科技,2017,33(7):245-253,230.FAN Li,XU Xiao-dong,SONG Ze,et al.Analysis of the key aroma-active compounds in braised pork[J].Modern Food Science and Technology,2017,33(7):245-253,230.
[10] 薛雁,周芳伊,黄峰,等.毛氏红烧肉特征风味成分分析[J].食品研究与开发,2019,40(11):153-158.XUE Yan,ZHOU Fang-yi,HUANG Feng,et al.Analysis of characteristic flavor components of mao's braised meat[J].Food Research and Development,2019,40(11):153-158.
[11] 赵越.红烧肉在加工和储藏过程中的品质变化研究[D].无锡:江南大学,2017.ZHAO Yue.Study on quality change of stewed pork during processing and storage[D].Wuxi:Jiangnan University,2017.
[12] 张泓,姚敏,黄峰,等.一种毛式红烧肉的制备方法：CN20150253992\[P\].2015-05-18.ZHANG Hong,YAO Min,HUANG Feng,et al.A preparation method of Mao-style roast pork:CN20150253992\[P\].2015-05-18.
[13] YANG Yang,ZHANG Xin,WANG Ying,et al.Study on the volatile compounds generated from lipid oxidation of Chinese bacon(unsmoked)during processing[J].European Journal of Lipid Science and Technology,2017,119(10):1600512(1-10).
[14] SHIBAMOTO T.Heterocyclic compounds found in cooked meats[J].Journal of Agricultural and Food Chemistry,1980,28(2):237-243.
[15] 唐琳,张春英.肉类的风味及其形成机制[J].山东师大学报(自然科学版),1996,11(2):74-78.TANG Lin,ZHANG Chun-ying.Flavor of meat and its formation mechanism[J].Journal of Shandong Normal University(Natural Science),1996,11(2):74-78.
[16] 刘登勇,赵志南,吴金城,等.基于SPME-GC-MS分析熏制材料对熏鸡腿挥发性风味物质的影响[J].食品科学,2019,40(24):220-227.LIU Deng-yong,ZHAO Zhi-nan,WU Jin-cheng,et al.Effects of different smoking materials on volatile flavor compounds in smoked chicken thighs[J].Food Science,2019,40(24):220-227.
[17] 马菲,郇延军,刁欣悦.酱制时间对传统酱卤猪肉制品风味及质构变化规律的影响[J].食品与机械,2019,35(9):55-63.MA Fei,HUANG Yan-jun,DIAO Xin-yue.Effect of sauce time on the flavor and texture change of traditional sauce and braised pork products[J].Food & Machinery,2019,35(9):55-63.
[18] LORENZO J M,DOMINGUEZ R.Cooking losses,lipid oxidation and formation of volatile compounds in foal meat as affected by cooking procedure[J].Flavor and Fragrance Journal,2014,29(4):240-248.
[19] SHOTA Tanimoto,KAORI Kitabayashi,CHIHIRO Fukusima,et al.Effect of storage period before reheating on the volatile compound composiion and lipid oxidation of steamed meat of yellowtail Seriola quinqueradiata[J].Fisheries Science,2015,81(6):1 145-1 155.
[20] 纪有华,王荣兰.红烧肉风味形成途径探讨[J].扬州大学烹饪学报,2006(2):19-23.JI Yuo-hua,WANG Lan-rong.Exploring the flavour formation pathways of braised pork[J].Culinary Science Journal of Ynagzhou University,2006(2):19-23.
[21] 王瑞澄,周芳伊,黄峰,等.毛氏红烧肉挥发性风味物质分析方法的建立[J].食品科技,2019,44(4):308-313.WANG Rui-cheng,ZHOU Fang-yi,HUANG Feng,et al.Establishment of analysis method for volatile flavor compounds in Mao red braised pork[J].Food Science and Technology,2019,44(4):308-313.
[22] JOSE DEL Pulgar,MAR Roldan,JORGE Ruiz-Carrascal.Volatile compound sprofile of sous-vide cooked pork cheeks as affected by cooking conditions(vacuum packaging,temperature and time)[J].Molecules,2013,18(10):125-138.
[23] 刘光宪,李雪,王丽,等.江西地方品牌酱鸭游离脂肪酸和风味特性分析[J].食品与机械,2021,37(1):53-60.LIU Guang-xian,LI Xue,WANG Li,et al.Analysis of free fatty acids and flavor characteristics of sauced duck from Jiangxi local brands[J].Food & Machinery,2021,37(1):53-60.
[24] LI Ning,ZHENG Fu-ping,CHEN Hai-tao,et al.Identification of volatilecomponents in Chinese Sinkiang fermented camel milk using SAFE,SDE,and HS-SPME-GC/MS[J].Food Chemistry,2011,129(3):1 242-1 252.
[25] 孙福犁,徐慢,崔和平,等.谷朊粉肽美拉德反应中间体的制备及风味形成能力研究[J].食品与机械,2019,35(3):1-7.SUN Fu-li,XU Man,CUI He-ping,et al.Preparation of Maillard reaction intermediates(MRIs)of gluten peptides-xylose and study on its flavor formation capacity[J].Food & Machinery,2019,35(3):1-7.
[26] WOOD J D,RICHARDSON R I,NUTE G R,et al.Effects of fatty acids on meat quality:A review[J].Meat Science,2003,66:21-32.