Abstract
bjective:The pyrolysis transfer rate of aglycones from 7 kinds of glucosides added to cigarette paper in mainstream and sidestream smoke was studied.Methods:5methylfurfuryl alcohol glucoside, menthol glucoside, anisyl alcohol glucoside, leaf alcohol glucoside, phenylethanol glucoside, ethyl vanillin glucoside and vanillin glucoside were applied to the surface of cigarette paper and inject into cigarette according to the 0.01% of the weight of cut tobacco respectively. The transfer rates of aglycones in mainstream smoke and side stream smoke were determined under two kinds of flavoring Methods. On this basis, the transfer rules of seven aglycones in mainstream smoke and sidestream smoke were studied when the concentration of 0.001%,0.010%and 0.050% was applied to cigarette paper.Results:In mainstream smoke, the transfer rates of seven aglycones in cut tobacco were higher than those added to cigarette paper, but the opposite was true in sidestream smoke; 5methylfurfuryl alcohol had the highest transfer rate of aglycones in mainstream smoke and sidestream smoke, and menthol had the lowest transfer rate, followed by leaf alcohol, anisyl alcohol, phenylethanol, ethyl vanillin and vanillin. Under the condition of 0.001% addition, the transfer rates of seven aglycones in mainstream and side stream smoke were 0.27%~1.24% and 0.42%~1.71% respectively,0.010%addition were 0.38%~1.87% and 0.54%~2.52% respectively, 0.050% addition were 0.31%~1.56% and 0.47%~2.19%respectively.Conclusion:The transfer rates of seven aglycones in side stream smoke were higher than those in mainstream smoke at three additive gradients, the transfer rates of aglycones in mainstream and side stream smoke showed a trend of first increasing and then decreasing with the increase of addition.
Publication Date
7-7-2022
First Page
16
Last Page
20
DOI
10.13652/j.issn.1003-5788.2022.02.003
Recommended Citation
Lu, HAN; Wen-juan, CHU; Shao-dong, HU; Zhi-wei, ZHAO; Jing, YANG; and Hai-ying, TIAN
(2022)
"Study on pyrolysis transfer rules of seven aglycones in flue gas under two kinds of flavoring Methods,"
Food and Machinery: Vol. 38:
Iss.
2, Article 3.
DOI: 10.13652/j.issn.1003-5788.2022.02.003
Available at:
https://www.ifoodmm.cn/journal/vol38/iss2/3
References
[1] 李欢,王建民,王豪礼,等.卷烟纸参数对卷烟持灰能力的影响[J].食品与机械,2021,37(6):207-212.LI Huan,WANG Jian-min,WANG Hao-li,et al.Influence of cigarette paper parameters on cigarette ash holding capacity[J].Food & Machinery,2021,37(6):207-212.
[2] 马胜楠,王建民,常冰冰,等.烟丝和卷烟纸中金属元素对自由燃烧速率的影响[J].食品与机械,2019,35(9):64-68.MA Sheng-nan,WANG Jian-min,CHANG Bing-bing,et al.Effects of metal elements on free burning speed in cutrag and cigarette paper[J].Food & Machinery,2019,35(9):64-68.
[3] 何红梅,张媛,朱怀远,等.抽吸模式对纸打孔细支卷烟烟气释放量的影响[J].食品与机械,2018,34(5):210-215.HE Hong-mei,ZHANG Yuan,ZHU Huai-yuan,et al.Effect of smoking regimes on smoke release of super slim cigarettes with perforation paper[J].Food & Machinery,2018,34(5):210-215.
[4] 祃志明,陈胜,熊国玺.含有黑香荚兰提取物的高档卷烟纸及其制备方法:CN2013103166930[P].2013-10-09.MA Zhi-ming,CHEN Sheng,XIONG Guo-xi.High grade cigarette paper containing black vanilla extract and its preparation method:CN2013103166930[P].2013-10-09.
[5] 徐朝阳,余红伟,陆刚,等.微胶囊的制备方法及应用进展[J].弹性体,2019,19(4):78-82.XU Chao-yang,YU Hong-wei,LU Gang,et al.Preparation and application of microcapsules[J].China Elastmerics,2019,19(4):78-82.
[6] 徐兰兰,王建民,刘朝富,等.微胶囊对卷烟纸阴燃速率和阴燃温度的影响[J].中国造纸,2020,39(5):87-90.XU Lan-lan,WANG Jian-min,LIU Chao-fu,et al.Effects of microcapsules on smoldering rate and burning temperature of cigarette paper[J].China Pulp & Paper,2020,39(5):87-90.
[7] 沈妍,徐兰兰,尧珍玉,等.微胶囊在卷烟用纸上的应用评价[J].中国造纸,2017,36(7):36-43.SHEN Yan,XU Lan-lan,YAO Zhen-yu,et al.Application of complex coacervation microcapsules in cigarette paper[J].China Pulp & Paper,2017,36(7):36-43.
[8] 秦艳,康林芝,云帆,等.沉香精油微胶囊的制备及其在卷烟纸中的应用研究[J].农产品加工,2016(7):9-16.QIN Yan,KANG Lin-zhi,YUN Fan,et al.Manufacturing microcapsules of eaglewood oil and application in cigarette paper[J].Farm Products Processing,2016(7):9-16.
[9] 卓浩廉,罗福明,伍锦鸣,等.红枣香精微胶囊的制备及其在卷烟纸中的应用研究[J].农产品加工,2015(7):17-18,22.ZHUO Hao-lian,LUO Fu-ming,WU Jin-ming,et al.Manufacturing microcapsules of zizyphusjujuba oil and application in cigarette[J].Paper Farm Products Processing,2015(7):17-18,22.
[10] 沈静轩,肖维毅,徐兰兰,等.苯乙醇微胶囊的稳定性及热释放行为研究[J].日用化学工业,2017,47(7):277-280.SHEN Jing-xuan,XIAO Wei-yi,XU Lan-lan,et al.Study on stability of phenethyl alcohol microcapsules and their thermal releasing behavior[J].China Surfactant Detergent & Cosmetics,2017,47(7):277-280.
[11] 黄富,刘斌,王平军.特色薄荷型卷烟纸的开发与应用[J].中国造纸,2012,31(1):42-44.HUANG Fu,LIU Bin,WANG Ping-jun.Manufacture of menthol cigarette paper[J].China Pulp & Paper,2012,31(1):42-44.〖HJ1.95mm〗
[12] 李炯,胡忠豪,王新年.一种清香型卷烟纸及其制备方法:CN105200857A[P].2015-12-30.LI Jiong,HU Zhong-hao,WANG Xin-nian.A kind of fresh cigarette paper and its preparation method:CN105200857A[P].2015-12-30.
[13] 刘斌,钟科军,朱效群,等.一种薄荷型卷烟纸的制备:CN2009100427133[P].2009-07-22.LIU Bing,ZHONG Ke-jun,ZHU Xiao-qun,et al.A kind of menthol cigarette paper and its preparation method:CN2009100427133[P].2009-07-22.
[14] 倪朝敏,王晓辉,李雪梅,等.一种蜜甜香型卷烟纸及其制备方法:CN2017109436522[P].2017-12-01.NI Chao-min,WANG Xiao-hui,LI Xue-mei,et al.A kind ofhoney sweet cigarette paper and its preparation method:CN2017109436522[P].2017-12-01.
[15] GREEN C R,COLLBY D A,COOPER P J,et al.Advances in analytical methodology of leaf and smoke[J].Adv Tob Sci,1980,6:123-183.
[16] HERRON J N.Tobacco product containing side stream smoke flavorant:US4804002[P].1989-02-14.
[17] CHAN W G.Smoking composition containing a flavorant-release saccharide additive:EP0506231[P].1996-09-11.
[18] 曾世通,刘珊,孙世豪,等.β-紫罗兰醇葡糖苷热裂解产物及其在卷烟主流烟气中的释放行为[J].烟草科技,2013(1):35-38.ZENG Shi-tong,LIU Shan,SUN Shi-hao,et al.Pyrolytic products of β-ionol-glucoside and their release behavior in mainstream cigarette smoke[J].Tobacco Science & Technology,2013(1):35-38.
[19] 毛多斌,周强,牟定荣,等.8种葡萄糖苷配糖体在卷烟主流烟气粒相物中的转移率测定[J].中国烟草学报,2012,18(l):1-5.MAO Duo-bin,ZHOU Qiang,MOU Ding-rong,et al.A study on transfer rates of main pyrolysis products of eight glycosides in mainstream cigarette smoke[J].Acta Tabacaria Sinica,2012,18(l):1-5.
[20] 李斌.潜香物质在低焦油卷烟香味补偿技术中的应用研究[J].安徽农业科学,2012(6):3 562-3 564.LI Bin.Application of flavor precursor in low-tar cigarette fragrance compensation[J].Journal of Anhui Agricultural Sciences,2012(6):3 562-3 564.
[21] 段海波,解万翠,姜黎,等.玫瑰醇-β-D-吡喃葡萄糖苷的卷烟增香及缓释作用[J].烟草科技,2019,52(4):57-64.DUAN Hai-bo,XIE Wan-cui,JIANG Li,et al.Application of rhodinol-β-D-glycoside in cigarette flavoring and slow aroma-releasing[J].Tobacco Science & Technology,2019,52(4):57-64.
[22] 解万翠,刘艺,阁威,等.糖苷类香料前体的卷烟加香和缓释效果[J].烟草科技,2006(7):40-42.XIE Wan-cui,LIU Yi,GE Wei,et al.Application of geranyl glycoside in cigarette flavoring[J].Tobacco Science & Technology,2006(7):40-42.
[23] 沈宏林.十六种烟用香料卷烟迁移行为研究[D].昆明:昆明理工大学,2009:38-43.SHEN Hong-lin.Research of transfer rate of sixteen flavors in cigarette blend[D].Kunming:Kunming University of Science and Technology,2009:38-43.
[24] 宋瑜冰,宗永立,谢剑平,等.一些酯类香料单体在卷烟中转移率的测定[J].中国烟草学报,2005,11(3):17-22.SONG Yu-bing,ZONG Yong-li,XIE Jian-pin,et al.The transfer ratio of some ester flavors in cigarett[J].Acta Tabacaria Sinica,2005,11(3):17-22.
[25] 李春,向能军,沈宏林,等.一些醛、酯类香料在卷烟中的转移率与卷烟焦油量的相关性研究[J].应用化工,2009,38(10):1 465-1 468.LI Chun,XIANG Neng-jun,SHEN Hong-lin,et al.Research on correlation of transfer ratio of some aldehydes and esters flavors and cigarettes tar content[J].Applied Chemical Industry,2009,38(10):1 465-1 468.
[26] 徐若飞,刘志华,陈章玉,等.一种盘纸添加剂的合成及热解分析[C]//2004年烟草化学学组年会论文集.广州:中国烟草学会,2004:221-223.XU Ruo-fei,LIU Zhi-hua,CHEN Zhang-yu,et al.Synthesis and pyrolysis analysis of an additive for paper tray[C]//Proceedings of the Annual Meeting of the Tobacco Chemistry Group.Guangzhou:China Tobacco Society,2004:221-223.