Abstract
Objective: This study aimed to obtain the volatile components of different parts of lavender in natural condition and provide theoretical basis for quality evaluation and rational utilization of lavender varieties.Methods: Orthogonal experiment was used to optimize the headspace solid phase microextraction (HS-SPME-GC-MS) conditions, and the volatile components of the root, stem, leaf and flower of the representative lavender species France blue were analyzed under the optimal conditions.Results: The optimal conditions of HS-SPME were extraction time 60 min, equilibrium time 20 min and desorption time 5 min. Under the control of these conditions, a total of 36 chemical components were identified from different parts of lavender, among which 6 compounds were identified from each part.Conclusion: The content of volatile components in different parts of lavender varies greatly, among which the content of volatile components in flower parts is higher than that in leaf, and the content of volatile components in stem and root is the least. The contents of ester compounds in flowers and stems were prominent. The contents of olefin in roots and leaves were more prominent.
Publication Date
10-16-2022
First Page
37
Last Page
42
DOI
10.13652/j.spjx.1003.5788.2022.90200
Recommended Citation
Guo-tong, CHEN; Yun, LU; Ping-ping, MA; Rui, FAN; Zhong, YANG; and Xu, CAO
(2022)
"Analysis of volatile components in different parts of lavender based on HS-SPME-GC-MS,"
Food and Machinery: Vol. 38:
Iss.
7, Article 6.
DOI: 10.13652/j.spjx.1003.5788.2022.90200
Available at:
https://www.ifoodmm.cn/journal/vol38/iss7/6
References
[1] 中国科学院中国植物志编辑委员会.中国植物志:第六十五卷:第二分册[M].北京:科学出版社,1977:248-250.Editorial Committee of Flora of China,Chinese Academy of Sciences.Flora of China:Volume 65:Volume 2[M].Beijing:Science Press,1977:248-250.
[2] 廖祯妮,黄青,程启明,等.云南两个薰衣草品种精油分析[J].天然产物研究与开发,2014,26(4):544-549.LIAO Zhen-ni,HUANG Qing,CHENG Qi-ming,et al.Chemicalcompositions of essential oils extracted from two cultivars of Lavandula spp.grown in Yunnan[J].Nat Prod Res Dev,2014,26(4):544-549.
[3] 陈燕,施玉格,李晨阳,等.狭叶薰衣草花与齿叶薰衣草花的比较研究[J].西北药学杂志,2017,32(5):541-544.CHEN Yan,SHI Yu-ge,LI Chen-yang,et al.Comparative study on flowers of Lavandula angustifolia Mill.and Lavandula dentata L.[J].North Pharm J,2017,32(5):541-544.
[4] 徐攀,王克柱,卢聪,等.薰衣草对神经系统药理作用的研究进展[J].现代药物与临床,2015,30(10):1 298-1 302.XU Pan,WANG Ke-zhu,LU Cong,et al.Research progress on neurological activities of Lavandula angustifolia[J].Drug & Clin,2015,30(10):1 298-1 302.
[5] 周广亮,宋晓琳,王志伟,等.薰衣草精油对HepG2细胞的抗增殖作用研究[J].食品工业科技,2013,34(8):158-160.ZHOU Guang-liang,SONG Xiao-lin,WANG Zhi-wei,et al.Study on anti proliferation effect of essential oil from the lavender on HepG2 cells[J].Food Ind Sci Tech,2013,34(8):158-160.
[6] EBRAHIMI H,MARDANI A,BASIRINEZHAD M H,et al.The effects of Lavender and Chamomile essential oil inhalation aromatherapy on depression,anxiety and stress in older community-dwelling people:A randomized controlled trial[J].Explore,2022,18(3):272-278.
[7] RIVAZ M,RAHPEIMA M,KHADEMIAN Z,et al.The effects of aromatherapy massage with lavender essential oil on neuropathic pain and quality of life in diabetic patients:A randomized clinical trial[J].Complementary Therapies in Clinical Practice,2021,44:101430.
[8] 李紫薇,张艺,张月梅,等.薰衣草花茶水提物的抗氧化活性研究[J].食品研究与开发,2013,34(1):28-30.LI Zi-wei,ZHANG Yi,ZHANG Yue-mei,et al.Antioxidant activity of water extracts from lavender tea[J].Food Research and Development,2013,34(1):28-30.
[9] 裴亚萍.不同季节薰衣草花精油挥发性香气成分的GC-MS分析及在花草茶饮料中的应用[J].中国食品添加剂,2018(3):142-147.PEI Ya-ping.The analysis of volatile compositions of Lavender oil at different seasons by GC-MS and its application in herbal tea beverage[J].Chin Food Add,2018(3):142-147.
[10] 童红,唐军,张正方.薰衣草及其精油的研究进展[J].香料香精化妆品,2013(6):55-58.TONG Hong,TANG Jun,ZHANG Zheng-fang.Study on theresearch development of lavender and its essential oil[J].Flav Frag Cosm,2013(6):55-58.
[11] 肖正春,张卫明,张广伦.薰衣草的开发利用与人类健康[J].中国野生植物资源,2015,34(2):63-66.XIAO Zheng-chun,ZHANG Wei-ming,ZHANG Guang-lun.Development of Lavandula L.and their benefits to human health[J].Chin Wild Plant Res,2015,34(2):63-66.
[12] 王强,施玉格,徐芳,等.比较研究新疆狭叶薰衣草不同部位挥发油成分[J].药物分析杂志,2013,33(3):404-408.WANG Qiang,SHI Yu-ge,XU Fang,et al.Comparative analysis on compositions of essential oil extracted from different parts of Lavandula angustifolia grown in Xinjiang[J].Chin J Pharm Anal,2013,33(3):404-408.
[13] 唐石云,申钦鹏,刘春波,等.用超临界流体萃取—气相色谱—质谱法分析薰衣草中挥发性化学成分[J].江西农业学报,2018,30(3):106-111.TANG Shi-yun,SHEN Qin-peng,LIU Chun-bo,et al.Determination ofvolatile chemical components in lavender by supercritical fluid extraction-gas chromatography-mass spectrometry[J].Acta Agri Jiangxi,2018,30(3):106-111.
[14] 童红,唐军.3种不同方法提取薰衣草挥发性成分的比较[J].中国实验方剂学杂志,2014,20(16):100-105.TONG Hong,TANG Jun.Analysis of volatile components from lavender by three different methods[J].Chin J Exp Tradit Med Form,2014,20(16):100-105.
[15] 徐洁华,孔辉,文首文,等.常温条件下薰衣草精气成分研究[J].林产化学与工业,2010,30(1):81-84.XU Jie-hua,KONG Hui,WEN Shou-wen,et al.Study oncomposition of phytoncidere from Lavandula angustifolia Mill.at room temperature[J].Chem Ind Forest Prod,2010,30(1):81-84.
[16] 赵洁,唐军,陈兆慧,等.薰衣草化学成分分析及差异标志物的识别[J].质谱学报,2016,37(6):517-525.ZHAO Jie,TANG Jun,CHEN Zhao-hui,et al.Identification ofchemical constituents and discrimination markers in lavender by HS-SPME-GC/MS[J].J Chin Mass Spectr Soc,2016,37(6):517-525.
[17] 陈国通,左书瑞,曹雪琴,等.吹扫捕集—气相色谱—质谱法测定薰衣草香气成分[J].安徽农业科学,2019,47(2):191-193.CHEN Guo-tong,ZUO Shu-rui,CAO Xue-qin,et al.Determination of aroma components of lavender by purge and trap-gas chromatography-mass spectrometry[J].J Anhui Agric Sci,2019,47(2):191-193.
[18] 赵杨,程力,杜庭,等.基于HS-SPME/GC/MS的姜花不同部位挥发性成分分析[J].食品与机械,2020,36(3):49-53.ZHAO Yang,CHENG Li,DU Ting,et al.Analysis on volatile components in different parts of Hedychium coroarium by HS-SPME/GC/MS[J].Food & Machinery,2020,36(3):49-53.
[19] 谢婧,徐俐,张秋红,等.顶空固相微萃取法提取菜籽油挥发性风味成分[J].食品科学,2013,34(12):281-285.XIE Jing,XU Li,ZHANG Qiu-hong,et al.Headspace solid phase microextraction of volatile flavor components from rapeseed oil[J].Food Sci,2013,34(12):281-285.
[20] 张鹏云,管维,李蓉,等.顶空—固相微萃取法与水蒸气蒸馏法提取山银花挥发性组分的比较[J].食品科学,2020,41(4):178-184.ZHANG Peng-yun,GUAN Wei,LI Rong,et al.Comparison of volatile components from flos lonicerae extracted by headspace solid phase microextraction and steam distillation[J].Food Sci,2020,41(4):178-184.
[21] ANGEROSA F,SERVILI M,SELVAGGINI R,et al.Volatile compounds in virgin olive oil:Occurrence and their relationship with the quality[J].Journal of Chromatography A,2004,1 054(1):17-31.
[22] TANKIEWICZ M,MORRISON C,BIZIUK M.Application and optimization of headspace solid-phase microextraction(HS-SPME)coupled with gas chromatography-flame-ionization detector(GC-FID)to determine products of the petroleum industry in aqueous samples[J].Microchemical Journal,2013,108:117-123.
[23] 初众,王海茹,张彦军,等.HS-SPME-GC-MS技术分析香草兰果皮的挥发性成分[J].食品科学,2016,37(6):126-131.CHU Zhong,WANG Hai-ru,ZHANG Yan-jun,et al.GC-MS analysis of volatiles in vanilla husk extracted by headspace solid-phase microextraction[J].Food Sci,2016,37(6):126-131.
[24] 白俊英,黄仁华,陆云梅,等.顶空固相微萃取—气相色谱—质谱联用分析费约果叶片挥发性香气成分条件优化[J].色谱,2016,34(8):778-782.BAI Jun-ying,HUANG Ren-hua,LU Yun-mei,et al.Optimization of headspace solid phase micro-extraction combined with gas chromatography-mass spectrometry conditions of volatile flavor from Feijoa sellowiana leaves[J].Chin J Chrom,2016,34(8):778-782.
[25] 张鹏云.六种药食同源物质挥发性成分的HS-SPME/GC-MS研究[D].广州:广东药科大学,2019:28.ZHANG Peng-yun.Study on the volatile components of six medicine and food homology substances by HS-SPME/GC-MC[D].Guangzhou:Guangdong Pharmaceutical University,2019:28.
[26] 张鹏云,李蓉,陈丽斯,等.顶空固相微萃取—气质联用法结合自动解卷积技术分析葛根中的挥发性成分[J].食品科学,2019,40(12):220-225.ZHANG Peng-yun,LI Rong,CHEN Li-si,et al.Analysis of volatile compounds in pueraria radix using headspace solid-phase microextraction-gas chromatography-mass spectrometry(HS-SPME-GC-MS)combined with automated mass spectral deconvolution and identification system(AMDIS)[J].Food Sci,2019,40(12):220-225.
[27] 王新玲,热娜·卡斯木,胡君萍,等.薰衣草不同部位中挥发油化学成分的比较[J].华西药学杂志,2010,25(3):361-362.WANG Xin-ling,KASIMU Re-na,HU Jun-ping,et al.Comparison of chemical components of volatile oils from the different parts of Lavandula angustifolia Mill[J].West Chin J Pharm Sci,2010,25(3):361-362.