Abstract
Objective: This study aimed to improve the yield and gelling property of lemon pectin. Methods: Oxalic acid was used to extract pectin from lemon residue. The factors of optimal ratio of solid-liquid, pH, extraction temperature and extraction time were optimized through single factor experiments and orthogonal experiments. The purity, degree of esterification and rheological properties of the extracted lemon pectin were analyzed. The differences of gelling property between the extracted lemon pectin and two kinds of commercial high methoxyl pectins (HMP-1, HMP-2) were compared. Results: The results showed that the yield of pectin extract was 22.83%, with total galacturonic acid of 76.06% and degree of esterification of 75.94%, when the ratio of solid-liquid was 1∶20 (g/mL), extracting pectin at pH 2.2 and 95 ℃ for 75 min. The viscosity of the extracted lemon pectin was higher than HMP-1 and HMP-2. The calcium sensitivity was between HMP-1 and HMP-2, and the temperature sensitivity was similar to HMP-2. The sol-gel transformation of the extracted lemon pectin was found at 76.55 ℃ in the calcium ion environment. Conclusion: Lemon pectin extracted by oxalic acid has good rheological and gel properties, and can be potentially used as a stabilizer in acidic milk drinks.
Publication Date
4-25-2023
First Page
182
Last Page
187
DOI
10.13652/j.spjx.1003.5788.2022.80372
Recommended Citation
Xi, ZHENG; Yan-jun-jie, ZOU; Mi-ya, ZHOU; and Xu, REN
(2023)
"Optimization and quality evaluation of extracting lemon pectin by oxalic acid,"
Food and Machinery: Vol. 39:
Iss.
2, Article 30.
DOI: 10.13652/j.spjx.1003.5788.2022.80372
Available at:
https://www.ifoodmm.cn/journal/vol39/iss2/30
References
[1] 陈晓梅, 曾晓房, 韩珍, 等. 柠檬渣综合利用研究进展[J]. 食品工程, 2018(2): 1-4.
[2] 张放. 全球柠檬来檬生产与鲜果贸易现状[J]. 中国果业信息, 2019, 36(8): 23-30.
[3] 黄莹星. 柠檬皮高酯果胶的分步提取及其性能研究[D]. 广州: 华南理工大学, 2020: 1-14.
[4] 何李, 李绍振, 高彦祥, 等. 柑橘属果皮渣制备膳食纤维的研究进展[J]. 食品科学, 2012, 33(7): 310-314.
[5] 唐清苗, 王鲁峰. 柑橘皮渣的功能组分及加工应用现状[J]. 食品与机械, 2022, 38(6): 180-185.
[6] 魏海香, 木泰华, 孙艳丽, 等. 果胶制备的研究进展[J]. 食品研究与开发, 2006(4): 157-160.
[7] 刘江. 柠檬果胶工艺制备及其在调配型酸性乳饮料中的应用研究[D]. 成都: 西华大学, 2020: 28.
[8] CHAN S, CHOO W S. Effect of extraction conditions on the yield and chemical properties of pectin from cocoa husks[J]. Food Chemistry, 2013, 141(4): 3 752-3 758.
[9] MORRIS V J, GROMER A, KIRBY A R. Architecture of intracellular networks in plant matrices[J]. Structural Chemistry, 2009, 20(2): 255-261.
[10] THEANDER O, WESTERLUND E, MAN P, et al. Plant cell walls and monogastric diets[J]. Animal Feed Science and Technology, 1989, 23(1/2/3): 205-225.
[11] PENG J, BU Z, REN H, et al. Physicochemical, structural, and functional properties of wampee (Clausena lansium (Lour.) Skeels) fruit peel pectin extracted with different organic acids[J]. Food Chemistry, 2022, 386: 132834.
[12] ZAHRA R, FARAMARZ K, MILAD K, et al. Optimization of microwave-assisted extraction and structural characterization of pectin from sweet lemon peel[J]. International Journal of Biological Macromolecules: Structure, Function and Interactions, 2020, 147: 1 107-1 115.
[13] EUN-HI C, HO-TAK J, BYUNG-HOO L, et al. Green process development for apple-peel pectin production by organic acid extraction[J]. Carbohydrate Polymers: Scientific and Technological Aspects of Industrially Important Polysaccharides, 2019, 204: 97-103.
[14] 李梦. 果胶酯化度的测定及凝胶流变性与分子结构关系研究[D]. 广州: 暨南大学, 2017: 2.
[15] LIN Y, AN F, HE H, et al. Structural and rheological characterization of pectin from passion fruit (Passiflora edulis f. flavicarpa) peel extracted by high-speed shearing[J]. Food Hydrocolloids, 2021, 114: 106555.
[16] 刘贺, 朱丹实, 徐学明, 等. 低酯桔皮果胶凝胶的动力学分析及分形研究[J]. 食品科学, 2008, 29(2): 76-81.
[17] 杨宇华, 徐晓斌, 黄佳艳. 响应面法优化超声波辅助提取沃柑皮中果胶工艺研究[J]. 中国食品添加剂, 2022, 33(4): 55-62.
[18] ZHOU P, ZHENG M, LI X, et al. A consecutive extraction of pectin and hesperidin from Citrus aurantium L.: Process optimization, extract mechanism, characterization and bio-activity analysis[J]. Industrial Crops and Products, 2022, 182: 114849.
[19] LAI J C H, MAHESAN D, BAINI R. Characterization and optimization of extracted pectin from unripe banana and mango fruit peels[J]. Materials Today: Proceedings, 2022, 65(7): 3 020-3 029.
[20] SHIVAMATHI C S, GUNASEELAN S, SOOSAI M R, et al. Process optimization and characterization of pectin derived from underexploited pineapple peel biowaste as a value-added product[J]. Food Hydrocolloids, 2022, 123: 107141.
[21] 王锦秀, 赵晴晴, 徐心怡, 等. 响应面优化超声波辅助酸法提取百香果皮果胶工艺及其抗氧化活性研究[J]. 食品工业科技, 2022, 43(13): 162-170.
[22] MADA T, DURAISAMY R, GUESH F. Optimization and characterization of pectin extracted from banana and papaya mixed peels using response surface methodology[J]. Food Science & Nutrition, 2022, 10(4): 1 222-1 238.
[23] 陈怡君, 王晓慧, 陈艳萍, 等. 响应面法优化超声波—微波协同辅助酸法提取猕猴桃皮果胶工艺及果胶理化性质分析[J]. 食品与发酵工业, 2022, 48(13): 238-246.
[24] 姚月华, 唐宁, 应熙锐, 等. 红萍多糖结构特征、流变特性及抗氧化活性[J]. 食品与机械, 2022, 38(3): 154-159.
[25] PICOT-ALLAIN M C N, AMIRI-RIGI A, ABDOUN-OUALLOUCHE K, et al. Assessing the bioactivity, cytotoxicity, and rheological properties of pectin recovered from citrus peels[J]. Food Bioscience, 2022, 46: 101550.
[26] 江杨. 苹果、山楂果胶性质研究及其在发酵乳中的应用[D]. 泰安: 山东农业大学, 2017: 32-36.
[27] 田芬, 王银娟, 欧凯, 等. 不同高酯果胶的钙敏特性及其对酸乳饮料稳定性的影响[J]. 食品工业科技, 2015, 36(19): 83-86.
[28] BEGUM R, AZIZ M G, YUSOF Y A, et al. Evaluation of gelation properties of jackfruit (Artocarpus heterophyllus) waste pectin[J]. Carbohydrate Polymer Technologies and Applications, 2021, 2: 244-251.
[29] 张苒. 柠檬皮果胶的理化特性及其稳定酸性乳饮料的研究[D]. 合肥: 合肥工业大学, 2019: 31-32.