Abstract
Objective: This study aimed to evaluate the determination uncertainty of four quinolones residues in honey by liquid chromatography-tandem mass spectrometry （LC-MS/MS）. Methods: Based on GB 31657.2—2021, a mathematical model for sources of uncertainty evaluation was established. The uncertainty of each variable which affect the result were calculated and the weight of each uncertainty component was assessed. Results: The uncertainties in the determination of enrofloxacin, sarafloxacin, ofloxacin and ciprofloxacin in honey were （4.97±0.81）, （10.13±1.58）, （7.67±1.23）, （14.97±2.25） μg/kg （P=95%，k=2） respectively. Conclusion: The main influencing factors of the determination uncertainty were preparation and dilution process of standard solution and fitting of standard curve, which should be controlled in practical work.
Publication Date
4-30-2024
First Page
75
Last Page
81
DOI
10.13652/j.spjx.1003.5788.2023.81288
Recommended Citation
Yun, YANG; Yang, CAO; Jing, LI; Feifei, ZHONG; and He, ZUO
(2024)
"Uncertainty evaluation for the determination of four quinolone residues in honey by liquid chromatography-tandem mass spectrometry,"
Food and Machinery: Vol. 40:
Iss.
3, Article 10.
DOI: 10.13652/j.spjx.1003.5788.2023.81288
Available at:
https://www.ifoodmm.cn/journal/vol40/iss3/10
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