Abstract
Objective: To investigate the differences in volatile odor substances of Cyclocarya paliurus tea from different origins. Methods: Taking Cyclocarya paliurus tea from Changde, Zhangjiajie, Shaoyang in Hunan, Xiushui in Jiangxi, Qiandongnan in Guizhou, and Enshi in Hubei as the research subjects, the gas chromatography-ion mobility spectrometry (GC-IMS) coupled with partial least squares discriminant analysis (PLS-DA) was used to investigate the characteristics of different volatiles and their similarities in green strychnine teas from different origins. Results: A total of 120 VOCs, including monomers of some substances and their polymers, were detected in Cyclocarya paliurus tea from different origins, which were 34 aldehydes, 21 olefins, 19 alcohols, 16 ketones, 10 esters, 8 carboxylic acids, 5 furans, 4 pyrazines, 2 ethers, and 1 benzene species, respectively. Among them, γ-pinene, styrene, 4-methyl-1-pentanol, and n-octanal were the main characteristic difference volatiles. Conclusion: There were some differences in the volatile organic compounds of Cyclocarya paliurus tea among different origins(P<0.05). It is possible to distinguish between different origins of cymbopogon tea based on the characteristic volatile substances. GC-IMS technology can effectively realize the origin identification and quality control of GC tea.
Publication Date
7-22-2024
First Page
161
Last Page
167,233
DOI
10.13652/j.spjx.1003.5788.2023.81014
Recommended Citation
Jie, LOU; Yaqian, ZUO; and Xing, TIAN
(2024)
"Characterization and analysis of the volatile components of Cyclocarya paliurus tea from different origins based on GC-IMS technology,"
Food and Machinery: Vol. 40:
Iss.
5, Article 23.
DOI: 10.13652/j.spjx.1003.5788.2023.81014
Available at:
https://www.ifoodmm.cn/journal/vol40/iss5/23
References
[1] SHEN Y B, PENG Y, ZHU X C, et al. The phytochemicals and health benefits of Cyclocarya paliurus (Batalin) Iljinskaja[J]. Frontiers in Nutrition, 2023, 6(10): 1158158.
[2] 陈絮蒙, 王雅靖, 陈靓, 等. 青钱柳活性物质及其代谢调节作用的研究与应用进展[J]. 食品与发酵工业, 2023, 49(12): 336-344.
CHEN X M, WANG Y J, CHEN L, et al. Research and application progress of active substances and their metabolic regulatory effects of Cyclocarya paliurus[J]. Food and Fermentation Industries, 2023, 49(12): 336-344.
[3] 王凯平, 李文蕊, 宋梦姿, 等. 青钱柳的化学成分、药理作用及产品开发研究进展[J]. 中国医院药学杂志, 2023, 43(18): 2 100-2 104.
WANG K P, LI W R, SONG M Z, et al. Research progress on chemical constituents, biological activities and product development of Cyclocarya paliurus[J]. Chinese Journal of Hospital Pharmacy, 2023, 43(18): 2 100-2 104.
[4] HE W,REN F, WANG Y Q, et al. Application of GC-IMS in detection of food flavor substances[J]. IOP Conference Series: Earth and Environmental Science, 2020, 545(1): 012030.
[5] 宋艺君, 庞来祥, 袁筱, 等. GC-IMS法比较不同酒龄猕猴桃酒特征香气物质差异[J]. 食品与生物技术学报, 2023, 42(2): 58-65.
SONG Y J, PANG L X, YUAN X, et al. Difference of specific aroma substances in kiwifruit wine of different ages compared by GC-IMS[J]. Journal of Food Science and Biotechnology, 2023, 42(2): 58-65.
[6] 王熠瑶, 张烝彦, 孙俊, 等. 基于GC-IMS技术分析糙米储藏过程中风味物质变化[J]. 食品与发酵工业, 2020, 46(6): 250-255.
WANG Y Y, ZHANG Z Y, SUN J, et al. Analysis of flavor changes of brown rice during storage based on gas chromatography-ion mobility spectrometry[J]. Food and Fermentation Industry, 2020, 46(6): 250-255.
[7] 金文刚, 陈小华, 耿敬章, 等. 基于气相—离子迁移谱分析不同产地“汉中仙毫”气味指纹差异[J]. 食品与发酵工业, 2021, 47(5): 231-237.
JIN W G, CHEN X H, GENG J Z, et al. Analysis of "Hanzhong Xianhao" odor fingerprints from different places based on GC-IMS[J]. Food and Fermentation Industry, 2021, 47(5): 231-237.
[8] QI H T, DING S H, PAN Z P, et al. Characteristic volatile fingerprints and odor activity values in different citrus-tea by HS-GC-IMS and HS-SPME-GC-MS[J]. Molecules, 2020, 25(24): 6 027.
[9] 倪瑞洁, 詹萍, 田洪磊. 基于GC-IMS结合多元统计方法分析炸制时间对花椒调味油挥发性物质的影响[J]. 食品科学, 2022, 43(6): 279-286.
NI R J, ZHAN P, TIAN H L. Effects of frying time on volatile flavor compounds in fried pepper (Zanthoxylum bungeanum) oil as analyzed by gas chromatography-ion mobility spectrometry and multivariate statistical analysis[J]. Food Science, 2022, 43(6): 279-286.
[10] 李湘, 江靖, 李高阳, 等. GC-IMS结合化学计量学分析不同采后处理对柑橘果皮挥发性化合物的影响[J]. 食品科学, 2021, 42(20): 128-134.
LI X, JIANG J, LI G Y, et al. Effects of different dostharvest treatments on volatile compounds in citrus peel analyzed by gas chromatography-ion mobility spectrometry combined with chemometrics[J]. Food Science, 2021, 42(20): 128-134.
[11] 鲁祥凯, 杨彪, 孙莹, 等. 基于GC-IMS的白酒特征分析及鉴别[J]. 中国食品学报, 2023, 23(1): 278-295.
LU X K, YANG B, SUN Y, et al. Feature analysis and identification of Baijiu based on gas chromatography-ion migration spectrometry[J]. Chinese Journal of Food Science, 2023, 23(1): 278-295.
[12] 丁云龙, 王浩东, 唐国玮, 等. 5种药食兼用菊花挥发性有机物的HS-GC-IMS与指纹图谱[J]. 食品与机械, 2022, 38(9): 52-58.
DING Y L, WANG H D, TANG G W, et al. HS-GC-IMS analysis and fingerprinting of volatile organic compounds in five species medicinal and edible Chrysanthemum morifolium Ramat[J]. Food & Machinery, 2022, 38(9): 52-58.
[13] 罗玉琴, 韦燕菊, 林琳, 等. 基于GC-IMS技术的福建白茶产地判别[J]. 农业工程学报, 2021, 37(6): 264-273.
LUO Y Q, WEI Y J, LIN L, et al. Origin discrimination of Fujian white tea using gas chromatography-ion mobility spectrometry[J]. Journal of Agricultural Engineering, 2021, 37(6): 264-273.
[14] 寇晓琳. 青钱柳茶主要特征性风味成分分析[D]. 南京: 南京林业大学, 2019: 18-19.
KOU X L. Analysis of main characteristic flavor components of Cyclocarya paliurus tea[D]. Nanjing: Nanjing Forestry University, 2019: 18-19.
[15] 夏和元, 杨玉莹, 张丹丹, 等. 采收时间及加工方式对青钱柳叶化学成分含量及抗氧化和降血糖活性的影响[J]. 湖北中医药大学学报, 2021, 23(1): 45-49.
XIA H Y, YANG Y Y, ZHANG D D, et al. Effects of harvest time and processing method on chemical components and antioxidant and hypoglycemic activities of Cyclocarya paliurus leaves[J]. Journal of Hubei University of Traditional Chinese Medicine, 2021, 23(1): 45-49.
[16] 张晓芹, 陈礼平, 王慧玉, 等. 不同产地青钱柳HPLC指纹图谱的建立[J]. 中国中医药科技, 2022, 29(3): 393-396.
ZHANG X Q, CHEN L P, WANG H Y, et al. Establishment of HPLC fingerprints of Cyclocarya paliurus from different origins[J]. China Traditional Chinese Medicine Science and Technology, 2022, 29(3): 393-396.
[17] 陈玮玲, 钟培培, 范琳琳, 等. 固相微萃取—气相色谱—质谱分析青钱柳叶挥发性成分[J]. 食品工业科技, 2016, 37(22): 52-58.
CHEN W L, ZHONG P P, FAN L L, et al. Analysis of volatile compounds in Cyclocarya paliurus leaves by SPME-GC-MS[J]. Food Industry Science and Technology, 2016, 37(22): 52-58.
[18] 汪荣斌, 秦亚东, 陈颖, 等. 化学计量学结合指纹图谱评价不同产地青钱柳叶的质量[J]. 中药材, 2018, 41(4): 917-921.
WANG R B, QIN Y D, CHEN Y, et al. Chemometrics combined with fingerprinting for evaluating the quality of leaves from different origins of Cyclocarya paliurus[J]. Chinese Materia Medica, 2018, 41(4): 917-921.
[19] 杨玉莹, 张丹丹, 罗心遥, 等. 指纹图谱及多成分定量结合化学模式识别法评价不同产地青钱柳质量[J]. 中草药, 2020, 51(4): 1 082-1 088.
YANG Y Y, ZHANG D D, LUO X Y, et al. Quality evaluation of Cyclocarya paliurus from different habitats by fingerprint and multi-component quantification combined with chemical pattern recognition[J]. Chinese Herbal Medicine, 2020, 51(4): 1 082-1 088.
[20] 甘爽, 陈志丹, 商虎, 等. 基于气相离子迁移谱技术的不同产地乌龙茶挥发性物质分析[J]. 食品与生物技术学报, 2022, 41(9): 68-77.
GAN S, CHEN Z D, SHANG H, et al. Analysis of volatile substance of oolong tea from different origins based on gas chromatography-ion mobility technique[J]. Journal of Food Science and Biotechnology, 2022, 41(9): 68-77.
[21] 龚霄, 陈廷慧, 胡小军, 等. 基于GC-IMS技术的百香果果啤风味分析[J]. 食品与机械, 2022, 38(11): 46-52.
GONG X, CHEN T H, HU X J, et al. Flavor analysis of passion fruit fruit beer based on GC-IMS technique[J]. Food & Machinery, 2022, 38(11): 46-52.