Abstract
[Objective] To improve the accuracy of online measurement of sugar content of grapefruit by near infrared spectroscopy. [Methods] The pomelo online non-destructive testing equipment developed by ourselves was used to collect diffuse transmission spectrum data of pomelo in three light regions. In the wavelength range of 650~950 nm, orthonormal variable transformation (SNV), multiple scattering correction (MSC), Normalize, Savitzky-Golay first order derivative, SG-1st preprocessed the original data, used the adaptive weighting algorithm (CARS) to screen the spectral characteristics of the grapefruit sugar content, and established a partial least squares regression (PLSR) model. 30 grapefruit samples that were not involved in the modeling were used for online verification. [Results] The modeling effect of light region C combined with SNV-CARS-PLSR method was the best. The coefficient of determination of the prediction set was 0.95 and the root-mean-square error was 0.30 °Brix. In online verification, the coefficient of determination was 0.90 and the root mean square error was 0.58 °Brix. The model had a strong ability to detect the sugar content of grapefruit on line. [Conclusion] The prediction model based on the spectral data collected under the condition that the light spot diameter is 70 mm and the light region C is 20 mm above the equator of the grapefruit can realize the online prediction of the sugar content of the grapefruit more effectively.
Publication Date
7-22-2024
First Page
124
Last Page
129
DOI
10.13652/j.spjx.1003.5788.2023.80681
Recommended Citation
Ziye, TANG; Tao, WEN; Xingyong, DAI; and Feng, HU
(2024)
"Research on influence of light region on near infrared spectroscopy for online detection of sugar content of grapefruit,"
Food and Machinery: Vol. 40:
Iss.
6, Article 17.
DOI: 10.13652/j.spjx.1003.5788.2023.80681
Available at:
https://www.ifoodmm.cn/journal/vol40/iss6/17
References
[1] 张立欣, 杨翠芳, 陈杰, 等. 基于变量优选的苹果糖分含量近红外光谱检测[J]. 食品与机械, 2021, 37(10): 112-118.
ZHANG L X, YANG C F, CHEN J, et al. Detection of sugar content in apple by near infrared spectroscopy based on variable optimization[J]. Food & Machinery, 2021, 37(10): 112-118.
[2] 徐晓. 苹果检测姿态与双点检测对苹果可溶性固形物含量可见/近红外光谱在线检测的影响研究[D]. 杭州: 浙江大学, 2019: 32-38.
XU X. Research about the influences of apple detection posture and double-point detection on online SSC determination for apples by Vis/NIR spectroscopy[D]. Hangzhou: Zhejiang University, 2019: 32-38.
[3] 沈懋生, 赵娟. 基于近红外光谱技术检测苹果气调贮藏期可溶性固形物含量[J]. 食品安全质量检测学报, 2022, 13(17): 5 495-5 503.
SHEN M S, ZHAO J. Detection of soluble solids content in apples during controlled atmosphere storage based on near-infrared spectroscopy[J]. Journal of Food Safety and Quality, 2022, 13(17): 5 495-5 503.
[4] LIU X W, WU X, LI G L. Optimized prediction of sugar content in 'Snow' pear using near-infrared diffuse reflectance spectroscopy combined with chemometrics[J]. Spectroscopy Letters, 2019, 52(7): 376-388.
[5] SUN T, LIN H J, XU H R, et al. Effect of fruit moving speed on predicting soluble solids content of 'Cuiguan' pears (Pomaceae pyrifolia Nakai cv. Cuiguan) using PLS and LS-SVM regression[J]. Postharvest Biology and Technology, 2008, 51(1): 86-90.
[6] 孟幼青, 翁海勇, 岑海燕, 等. 潜伏期柑橘黄龙病宿主糖代谢及近红外光谱特征[J]. 浙江农业学报, 2019, 31(3): 428-435.
MENG Y Q, WENG H Y, CENG H Y, et al. Carbohydrate metabolism and near-infrared spectral characteristics in asymptomatic Huanglongbing infected leaves[J]. Acta Agriculturae Zhejiangensis, 2019, 31(3): 428-435.
[7] 张欣欣, 李尚科, 李跑, 等. 近红外光谱的不同产地柑橘无损鉴别方法[J]. 光谱学与光谱分析, 2021, 41(12): 3 695-3 700.
ZHANG X X, LI S K, LI P, et al. A nondestructive identification method of producing regions of citrus based on near infrared spectroscopy[J]. Spectroscopy and Spectral Analysis, 2021, 41(12): 3 695-3 700.
[8] 孙通, 莫欣欣, 刘木华. 果皮对脐橙可溶性固形物可见/近红外检测精度的影响[J]. 光谱学与光谱分析, 2018, 38(5): 1 406-1 411.
SUN T, MO X X, LIU M H. Effect of pericarp on prediction accuracy of soluble solid content in navel oranges by visible/near infrared spectroscopy[J]. Spectroscopy and Spectral Analysis, 2018, 38(5): 1 406-1 411.
[9] 宋杰. 基于脐橙位置状态分类识别的可溶性固形物在线检测研究[D]. 重庆: 西南大学, 2020: 91-115.
SONG J. Research of online detection of soluble solids content in navel orange based on position classification[D]. Chongqing: Southwest University, 2020: 91-115.
[10] POREP J U, MRUGALA S, MARTIN S, et al. Online determination of ergosterol in naturally contaminated grape mashes under industrial conditions at wineries[J]. Food and Bioprocess Technology, 2015, 8: 1 455-1 464.
[11] 姜小刚, 朱明旺, 姚金良, 等. 基于近红外在线装置苹果糖度模型参数优化研究[J]. 光谱学与光谱分析, 2023, 43(1): 116-121.
JIANG X G, ZHU M W, YAO J L, et al. Research on parameter optimization of apple sugar model based on near-infrared on-line device[J]. Spectroscopy and Spectral Analysis, 2023, 43(1): 116-121.
[12] QI S Y, OSHITA S, MAKINO Y, et al. Influence of sampling component on determination of soluble solids content of Fuji apple using near-infrared spectroscopy[J]. Applied Spectroscopy, 2017, 71(5): 856-865.
[13] 李雄, 刘燕德, 欧阳爱国, 等. 基于近红外的柚子品种判别和糖度检测通用模型[J]. 发光学报, 2019, 40(6): 808-814.
LI X, LIU Y D, OUYANG A G, et al. A general model for judging and brix detection of grapefruit variety based on near infrared[J]. Chinese Journal of Luminescence, 2019, 40(6): 808-814.
[14] TIAN H, XU H R, YING Y B. Can light penetrate through pomelos and carry information for the non-destructive prediction of soluble solid content using Vis-NIRS?[J]. Biosystems Engineering, 2021, 214(2 020): 152-164.
[15] JIE D F, ZHOU W H, WEI X. Nondestructive detection of maturity of watermelon by spectral characteristic using NIR diffuse transmittance technique[J]. Scientia Horticulturae, 2019, 257: 108718.
[16] JIE D F, XIE L J, RAO X Q, et al. Using visible and near infrared diffuse transmittance technique to predict soluble solids content of watermelon in an on-line detection system[J]. Postharvest Biology and Technology, 2014, 90: 1-6.
[17] 王世芳, 韩平, 崔广禄, 等. SPXY算法的西瓜可溶性固形物近红外光谱检测[J]. 光谱学与光谱分析, 2019, 39(3): 738-742.
WANG S F, HAN P, CUI G L, et al. The NIR detection research of soluble solid content in watermelon based on SPXY algorithm[J]. Spectroscopy and Spectral Analysis, 2019, 39(3): 738-742.
[18] 孙潇鹏, 刘灿灿, 陆华忠, 等. 基于可见—近红外透射光谱的蜜柚检测中影响因素分析[J]. 包装与食品机械, 2022, 40(4): 1-7.
SUN X P, LIU C C, LU H Z, et al. Analysis of influencing factors in the detection of honey pomelo based on visible-near infrared transmittance spectroscopy[J]. Packaging and Food Machinery, 2022, 40(4): 1-7.
[19] 孙潇鹏, 刘灿灿, 陆华忠, 等. 基于近红外透射光谱与机器视觉的蜜柚汁胞粒化分级检测[J]. 食品科学技术学报, 2021, 39(1): 37-45.
SUN X P, LIU C C, LU H Z, et al. Detection of honey pomelo in different granulation levels based on near-infrared transmittance spectroscopy combined with machine vision[J]. Journal of Food Science and Technology, 2021, 39(1): 37-45.
[20] WORKMAN J. Practical guide to interpretive near-infrared spectroscopy[J]. Angewandte Chemie, 2008, 47(25): 4 628-4 629.